超純水的取水方法，對分析實驗所造成的影響？
傳統上，超純水系統在非取水狀態時，由於系統的運作停止，會造成系統內超純水停滯而使水質劣化。為了防止停滯現象發生，較先進的超純水系統，在非取水期間仍能定期進行系統內部循環，以維持最佳超純水的狀態。但由於系統內部循環無法延伸到最終過濾膜上，成為超純水系統中唯一的滯留部分。而取樣口由於經常與外界空氣接觸，所以最終濾膜便成為水質劣化的主因。
圖１至圖４為超純水系統停止運作24小時後進行連續取水，檢測所取出的超純水在TOC值、金屬離子濃度、陰離子濃度與內毒素濃度的變化情形。當超純水系統中的比阻抗值達18.2MΩ‧cm後，便開始取水。結果顯示，前述取水初期的檢測數值都非常的高。這表示，經過夜間長時間無人取水情況下，初期所採得的水質有明顯劣化的現象。推測其原因，最終濾膜所造成的超純水滯留，以及取樣口與外界空氣接觸而造成水質污染等兩項主因。這時候只要將取水初期的數百毫升至1公升的純水排掉後，其後就可以將污染物質的濃度降到最低。
因此，我們從停止運作24小時的超純水系統做取水比較，將取水初期與排水1L後的超純水進行HPLC分析。我們可以發現，停止運作後初期採得的超純水，除了有較高的背景值外，HPLC分析圖含有數個波峰。而排水1L後的水質，則具有穩定的背景值。也就是，超純水取水時一定要將初期出水放掉，以獲得較安定的水質（圖５）。
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